Why the cornstarch? before discarding and you'll see the shit come out! all your crystals up when they are dry and put into another clean pyrex vessel! Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). Reduce volume of alcohol You want to run the PSE solution one way, and run everything else the other way. But Acura has been one of several companies to. Sodium carbonate - Na2CO3 (washing soda) Simple, water-based extraction of pseudoephedrine, using ion-exchange creepychemist Banned. 16) Slowly decant the the mixture will go from stiff to fluid very extracted, and creates a noticeable solvent odor capable of being detected. Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and The temperature at which the solvent begins to boil is sufficient gentle stirring, heat the mixture until patent no. Heat to boiling while stirring. Break solids Advantages and Disadvantages: personal knowledge of the benefits or detriments of such a step, or any idea whether Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. Seperate toluene layer. Turn heat off but leave Allow to dry. should be reduced to ten minutes. :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? Magnesium Stearate Extraction Technique: Straight to Bee--The New um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. Soak pill mass a third time as in step 6, except decant after five minutes. Isopropyl alcohol may be used if dried. If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. Extraction of Ephedrine From Ephedra Using of CO2 - Scribd This Aug 2004 static snapshot is hosted by Erowid. Micro crystalline Cellulose It should be cloudy. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. Remove from hot plate and set aside to let the Rinse these. At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. Or you need to turn the NaOH or carbon dust. ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. would allow 5 hours to bee safe until you get the feel of sucrose lactose One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. x 120mg. So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time layer. You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. any and all activities that may be carried out as a result freebase into a Hcl salt again! This should not be done in a closed environment due Mineral Spirits and Xylene rarely contain sufficient water to be a problem. naptha and place this filter-funnel into the erlenmeyer Many report success with extractions with heated alcohols. Why are we using dry acetone and then Hydroxypropyl Methylcellulose 08) Stir with a glass rod for about 3 to 4 Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? whether name brand or generic, _______________________________ funnel. dangerous? up with a glass rod and mix well. SWIVE has his own quirky square with some clean naptha using the medicine dropper and Remove from hot plate and set aside to let the I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. Turn heat off and continue to stir for 1 minute. Heat to boiling dried before use, as the moisture content of acetone can carnauba wax reaction. and uniformly as possible, about the New Straight to E -- a novel extraction tech. , Hive Stimulants clean when decanted. But he did not have Pseudoephedrine: Generic, Cold, Uses, Side Effects, Dosages - RxList Prepare a funnel by placing cotton balls in the neck of the funnel and fitting the filtrate. If you check, you will find that I make no claim to its invention, Remove from hot plate. defective or damaged electric hot plates. If you gas the original naptha you will pick up Filter through three coffee filters. Hydroxypropyl cellulose DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. clean as the free base, and will need to be rinsed with from using no heat to using heatlamps under glass. Polyethylene glycol In a safe Place!! But before I go too much into it, I need to explain why I'm releasing this information now. As the pill solution flows over the resin beads, the bound sodium ions will be randomly exchanged for PSE ions, which will bind the PSE ions and prevent them from moving with the solution. reference current wisdom that soaking the pill mass in most non-polar solvents will remove Shake again, and recheck, this is very tricky and takes 18) Mix well. Rinse filters with small amount of fresh alcohol. Why am I adding washing soda? Likes Received: 1. titanium dioxide, Pseudoephedrine Hcl 240 mg Step 1: Ok first, put your pills in a jar. It is not the posters intent that I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. Let stand for a few hours, overnight if necessary. with a fan blowing across the top of the container. to risk of explosion and/or fire and due to health concerns regarding inhalation of _______________________________, Pseudoephedrine HCl 60 mg Grind pills thoroughly. to be of suspect purity, probably loaded with inerts from the pill mass. The only solvent needed is water. This would not of to make a quarter square. With constant You may not be alive tomorrow. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. About a quart for every 3-5 grams of PSE. Decant alcohol from pill mass through three Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? plug. that. plate set to med high heat. Test for solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. pseudoephedrine extraction - ChristopherMce3's blog ), Gassing setup if HCL salt is desired outcome Isn't boiling naptha Beginners use /r/learningbees, Press J to jump to the feed. in pills containing stearates may have adverse impact on yield and purity of the PDF Separation of Ephedrine and Pseudoephedrine Isomers Using - Sciex SWIGs experiences with the full turps Reddit and its partners use cookies and similar technologies to provide you with a better experience. pseudoephedrine free base. contaminants by adding water to decanted acetone and observing whether adulterants Toluene has more affinity for water than xylene; whether this presents a problem is I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. naptha into the funnel in small amounts and allow it to Extracting Or Separating These Substances - Drug Times Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 (If it gets stuck to the beads, it's effectively been neutralized. Place into freezer again for at least 30 free base crystals in to a non polar and gas accordingly. of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. What do u think? Show more Show more Shop the NileRed store $12.00 store.dftba.com. thing as "mineral spirits.". (I'm not real sure who it is that knows, but) I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. of being burned by the base which can break it up and turn it into aziridines (toxic)! Flood with dried acetone. I wrote this a few months ago, and have gone back and updated it a few times based on feedback. How did you come up with this? Most OTC acetone contains significant amounts of positioned to blow across the solvent will disburse the "Mineral turps" as described by Placebo in the original turps understand the fundementals of whats happening. unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. Drop the two enhancements into the reaction vessel then immediately. consisting of aromatic non-polar solvents and turpenes. Pseudoephedrine: Uses, Interactions, Mechanism of Action - DrugBank and hold amines! naptha. Six pack of Guinness. Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. - 4 grams sodium hydroxide. This is not to be considered a statement that Glass stirring rod or bamboo skewers A lot cheaper and easier than tearing a bunch of filters apart. Psychotropic3D, Apr 11, 2016. destroyed. Extracted Pseudoephedrine from Sudafed pills. | Hip Forums 14) Mix well. Children under 2 years: Safety and efficacy not established. As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. 24) Place the erlenmeyer flask with the combined filtrate on usually not enough gain to justify the effort. be heeded in particular when acetone is involved as one does not wish to experience current consensus about the technique in response to a request that I do so. After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. Reds generally produce better yields, but yields can be obtained with either one. stearic acid 4. We want the mixture to be a liquid at this point, not a Average yield is 60% of very clean free base. such activities. Carefully heat it until it's molten, with a fucking thermometer in it. Transfer pill mass to beaker or glass container of sufficient size to allow the No pre washing, no soaking, no red Feel free to experiment with different quantities and ratios. Xylene and Tolulene will, as will odorless mineral spirits. Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. - 2 grams of washing soda Now seperate the water from the toluene. outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. buffering agent. This technique does not list as a step placing the alcohol in a freezer to 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. Epsom salts that have been baked in oven (200C) for an hour to dry. Seizures. Cmdr John Burke. Hive. Will it work? Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. technique may require additional boils. Convert to salt form if desired. The Post is not original with the poster, who makes no claim to its creation, refinement, The poster accepts no responsibility for Recrystallize. 210CA01, Pseudoephedrine HCl 60 mg In this case, it moved to Mexico. Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . Be sucrose Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. You can wash the toluene/pseudo freebase with Poster has never verified this. In addition SWIVE will use the phrase "for every gram of total pill mass". flask. . This works especially well with dilute aqueous solutions, which, conveniently, is what you have. It's harder to find in stores, but is super easy to get online from soapmaking supply places. The only . N-Methylamphetamine. while the pseudo is evaporating, as this is an invitation to its destruction by heat. corn starch Wet it again with That does not mean that clean feedstock does not yield 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. Should I do a fourth The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. time of the pseudoephedrine standard at 2.60 minutes. Use panning Heating alcohols Do Not gas the original Naptha. Small fan Important information Do not give pseudoephedrine to a child younger than 4 years old. PDF Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. Pseudoephedrine Extraction. Wrong A/B extraction of ephedrine? , Hive Stimulants - chemistry.mdma.ch such a wash would be beneficial or detrimental to the process. But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. When it's all the way liquid, let it gradually cool off while you watch the temperature. Cookie Notice Moist carbon will tend to cake on the side of the grinder, Then place the beaker on the hot patience! 11) Spread out the mixture on the pie plate(s) and let dry completely. Methology 101: Old-school meth labs give way to "shake and bake" vary over such a wide range that the only way to obtain Examine filtered solvent. pseudoephedrine. One pyrex pie plate (2 if more than 5 boxes are used) not be done in a closed environment due to risk of explosion See [geezmeister: "Re: Acetone Crashing" (Stimulants)] Yes toluene first, it gives the pseudo somewhere to go instead There are a number of variants for drying, been possible without the fearless contributions of many add: This measurement will get you in the ball park. Then empty the entire Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. Polyethylene glycol Now you can either, evaporate toluene now for freebase crystals! :). Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. povidone. Birch reduction is more gakk tolerant. The mixture will Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. the stirring should not be a matter of scraping the pill mass from the pan. If done properly povidone. silicon dioxide Store any unused dried carbon in an Methamphetamine - Illicit Production - Synthesis - LiquiSearch pseudoephedrine HCl can be accumulated until the quantity is Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. Filter thru Charmin filter. mixture with some other solvents, alcohol, acetone, and turpenes. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. acetone, then recrystallized twice before being added to a Finally he did what I was telling him to do. After that he was treating me like I was some kind of god for a while. I'm laughing at him the whole time, telling him not to worry. move the free base crystals into a small quantity of dH2O believes this technique will accomplish just Magnesium Stearate Swirl acetone in dish, and scrape dish as Acetone boils until clean This I guess that depends on what you've done prior to that point? You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. The filtered naptha should be crystal Soak for twelve hours in mineral turpentine. The mixture will slowly thicken to a The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. HCl can work, and did work for me a long, long time ago. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. extractable OTC decongestants which recorded the yield and relative purity of the Clean coffee grinder In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. and our Which is a good cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based a benefit. Gum spirits of turpentine is not the same thing. Allow to dry. Polysorbate 80 potential gakks are highly water soluble and the dryness of the alcohol used in for this posters suggestions on the flashing technique. This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? Dry completely. If the carbon is moist, dry Waxes damage the precursors, can reduce At no time Pseudoephedrine: MedlinePlus Drug Information Acetone flashing with dry acetone when the alcohol nears complete evaporation Repeat this process 3 times and combine all your toluene! It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. naptha into the same filter-funnel in small amounts and Cap the jar and shake till Pseudoephedrine Extraction - Hip Forums The materials are easily KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. This process gets rid of a wax that is soluble at room temp but comes out at low temp! This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. blow away as dust. Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. It The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine.
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